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This thesis addresses the development of a new force spectroscopy tool, correlation force spectroscopy (CFS) for the measurement of the properties of very small volumes of material (molecular to m3) at kHzMHz frequency range. CFS measures the simultaneous thermal fluctuations of two closelyspaced atomic force microscopy (AFM) cantilevers. CFS then calculates the crosscorrelation in the thermal fluctuations that gives the mechanical properties of the matter that spans the gap of the two cantilevers. The book also discusses development of CFS, its advantages over AFM, and its application in single molecule force spectroscopy and microrheology.
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