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Understanding of the molybdenum diselenide formation is important for the development of low resistance electrical back contacts for high efficiency solar cells, since thickness and crystallographic orientation of molybdenum diselenide layer determine the adhesion and electrical properties of the absorberMo interface. This book focuses on the selenization process of Mo samples prepared by different methods and different coverages: sputtered glass/Mo, Mofoil, glass/ITO/Mo, glass/Mo/In, glass/Mo/Cu, glass/Mo/CuIn and glass/Mo/CuZnSe were used as substrates to study the molybdenum diselenide layer formation. Dependence of the selenization process of Mo on the temperature and time was studied by the twotemperature zone and the isothermal onezone selenization methods. Thickness, structure, morphology and composition of molybdenum diselenide were determined. Samples were characterized by EDX, SEM, XRD, XPS, Raman and by the Hot Probe method.
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