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If you have any questions, you are always welcome to contact us. We'll get back to you as soon as possible, withing 24 hours on weekdays.
Customer service
All questions about your order, return and delivery must be sent to our customer service team by e-mail at yourstore@yourdomain.com
Sale & Press
If you are interested in selling our products, need more information about our brand or wish to make a collaboration, please contact us at press@yourdomain.com
A novel methodology has been described, employing the RambergBcklund rearrangement to synthesize Cglycosides. The RambergBcklund sequence to provide Cglycosides includes three intermediates: thioglycoside, sulfonyl glycoside, and exoglycal. Thioglycosides can be easily made using different methods. Sulfone formation was routine with MMPP. The onepot RambergBcklund reaction of sulfone was done using C2Br2F4 , tBuOH and KOH/Al2O3 under reflux to afford an exoglycal intermediate. The beltaCglycosides can be made by hydrogenolysis of exoglycals using H2 and Pd/C. The alphaCglycosides can be made stereoselectively from exoglycals via intramolecular ionic hydrogenation as the key step. Some of the C glycerolipids that have been prepared exhibit strikingly similar in vitro antiproliferative effects to those of Oglycoside analogs.
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